Direct observation of reduction of PdO to Pd metal by in situ electron microscopy

Peter Crozier; Abhaya K. Datye

doi:10.1016/s0167-2991(00)80501-7

Direct observation of reduction of PdO to Pd metal by in situ electron microscopy

Peter Crozier, Abhaya K. Datye

Materials Science and Engineering

Research output: Contribution to journal › Article › peer-review

19 Scopus citations

Abstract

We have made direct in situ observations of the reduction of small particles of PdO to Pd metal using electron microscopy. We find that the reduction at low temperature (<500°C) proceeds via the formation of a metal shell surrounding an oxide core. Complete reduction leads to the production of metal particles containing central voids.

Original language	English (US)
Pages (from-to)	3119-3124
Number of pages	6
Journal	Studies in Surface Science and Catalysis
Volume	130 D
DOIs	https://doi.org/10.1016/s0167-2991(00)80501-7
State	Published - 2000

ASJC Scopus subject areas

Catalysis
Condensed Matter Physics
Physical and Theoretical Chemistry
Surfaces, Coatings and Films
Materials Chemistry

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10.1016/s0167-2991(00)80501-7

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title = "Direct observation of reduction of PdO to Pd metal by in situ electron microscopy",

abstract = "We have made direct in situ observations of the reduction of small particles of PdO to Pd metal using electron microscopy. We find that the reduction at low temperature (<500°C) proceeds via the formation of a metal shell surrounding an oxide core. Complete reduction leads to the production of metal particles containing central voids.",

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doi = "10.1016/s0167-2991(00)80501-7",

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AU - Crozier, Peter

AU - Datye, Abhaya K.

PY - 2000

Y1 - 2000

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AB - We have made direct in situ observations of the reduction of small particles of PdO to Pd metal using electron microscopy. We find that the reduction at low temperature (<500°C) proceeds via the formation of a metal shell surrounding an oxide core. Complete reduction leads to the production of metal particles containing central voids.

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U2 - 10.1016/s0167-2991(00)80501-7

DO - 10.1016/s0167-2991(00)80501-7

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SN - 0167-2991

VL - 130 D

SP - 3119

EP - 3124

JO - Studies in Surface Science and Catalysis

JF - Studies in Surface Science and Catalysis

ER -

Direct observation of reduction of PdO to Pd metal by in situ electron microscopy

Abstract

ASJC Scopus subject areas

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