Replication Data for: In situ Raman Spectroscopy of Microwave Synthesis of Inorganic Compounds

TiO2 anatase to rutile proof-of-concept study In situ Raman spectroscopic data for the observation of a phase change in TiO2 (titania) from anatase to rutile. These data sets are the results of a proof-of-concept study for a custom Raman instrument which was built for the purpose of observing inorganic transformation under microwave heating and at high temperatures in the standard synthetic laboratory environment. They demonstrate the ability of the new instrument to observe these transformations in real-time and gain a better understanding of microwave heating methods for inorganic synthesis. It is relevant to Raman spectroscopists and inorganic synthetic chemists, especially those specializing in microwave processing. Dataset contains 7 delimited data files (.csv, .tab) and 6 MATLAB live scripts (.mlx). See README for additional information.